Advanced Gas Chromatography

with Matthew Klee
Tuesday, April 17, 2018 - Wednesday, April 18, 2018
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About This Course

Day 1

  1. Capillary GC tune-up (Myth Busters)

    1. Common myths and misconceptions debunked – things you were taught as “best practices” that have since been proven inferior

    2. Current best practices

  2. Sample introduction – advanced techniques

    1. Large volume injection

    2. Gentle approaches (PTV, COC)

  3. Fast GC – Method Translation

    1. how to painlessly and quickly migrate your current methods

    2. Compromises/tradeoffs

  4. Enablers (Capillary Flow technology)

    1. Connections

    2. Splitters

    3. Switches

  5. Capillary column backflush

 

Day 2

  1. Multidimensional GC Separations

    1. Heartcut multidimensional separations (instrumentation, practice)

      1. When, why, how

    2. GCxGC

      1. Reality vs. hype

      2. Modulators

      3. Initial method choices

      4. Optimization

  2. Optimal Capillary GC/MS

    1. Staying out of trouble

    2. Maximizing performance

  3. Method development and troubleshooting - interactive discussion a la CFDV

    1. Attendee problems are discussed in guided open forum format. Bring details to share. Benefit from the collective experience of your fellow classmates and the instructor.

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